Lithium iodide → HCID 66874398, compound

Participants

Reaction Steps

To a solution of lithium iodide (185 mg, 1.38 mmol) in refluxing anhydrous pyridine (10 mL) was added methyl 2-((2S,6S)-2,6-dimethylpiperazin-1-yl)benzoxazole-4-carboxylate (100 mg, 0.346 mmol) and the reaction mixture was refluxed for 24 hours. The mixture was cooled to room temperature, concentrated to dryness and dried in vacuo to provide lithium 2-((2S,6S)-2,6-dimethylpiperazin-1-yl)benzoxazole-4-carboxylate as a solid which was used without further purification: MS consistent

Provenance & Evidence