HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 58087452, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 3-[(Propane-1-sulfonyl)amino]benzoic acid | HCID 16228262 | — |
| Product | HCID 58087452 | HCID 58087452 | — |
Reaction Steps
A solution of 3-(propane-1-sulfonylamino)-benzoic acid (76, 1.20 g, 4.93 mmol) in thionyl chloride was heated to reflux for 3.0 hours. Evaporation of the solvent gave compound 77 as white solid that was used for the next step.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07863288B2 |
| Source dataset | uspto-grants-2011_01 |
| ORD ID | ord-5e4920dd7bd545bf8e68f5ef11f5b345 |
| Source note | uspto-grants-2011_01 |