HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → HCID 58086875, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | 1H-Pyrrolo(2,3-b)pyridine | HCID 9222 | — |
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Reactant | 4-(Benzyloxy)-3-methoxybenzaldehyde | HCID 75506 | — |
| Product | HCID 58086875 | HCID 58086875 | — |
Reaction Steps
Methanol (125 mL) and potassium hydroxide (4.4 g, 79 mmol) were mixed with 1H-pyrrolo[2,3-b]pyridine (94, 3.1 g, 26.6 mmol) and 4-benzyloxy-3-methoxy-benzaldehyde (564, 12.9 g, 53.2 mmol). The reaction was stirred at room temperature for 2 days. The resulting white solid was filtered and washed with water. Crude material was carried forward without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07863288B2 |
| Source dataset | uspto-grants-2011_01 |
| ORD ID | ord-9ed37c67425f4cfea452a6070c51d516 |
| Source note | uspto-grants-2011_01 |