HuagongsheHuagongshe Chemistry Print Report · For research reference only
Isobutylamine → HCID 86067101, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Isobutylamine | HCID 6558 | — |
| Reactant | HCID 57758083 | HCID 57758083 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 86067101 | HCID 86067101 | 90% |
Reaction Steps
Add isobutylamine (8.7 mL) dropwise to a solution of N-[methyl]-N-[methoxy]-3-fluoro-4-nitrobenzamide (2 g, 8.77 mmol) in 80 mL dry acetonitrile at 0° C. Stir the resulting orange solution at room temperature over night. Concentrate under reduced pressure to provide the desired compound (90%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07863310B2 |
| Source dataset | uspto-grants-2011_01 |
| ORD ID | ord-c86c433a2cee4afc9150c90fcaf4ff36 |
| Source note | uspto-grants-2011_01 |