HuagongsheHuagongshe Chemistry Print Report · For research reference only
tert-Butyl (3-aminopropyl)carbamate → HCID 67271831, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | tert-Butyl (3-aminopropyl)carbamate | HCID 2735700 | — |
| Reactant | Sodium borohydride | HCID 4311764 | — |
| Reactant | 3,5-Dimethylpyridine-2-carbaldehyde | HCID 18731683 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 67271831 | HCID 67271831 | — |
Reaction Steps
Using General Procedure B: Reaction of (3-aminopropyl)-carbamic acid tert-butyl ester and 3,5-dimethylpyridine-2-carboxaldehyde in anhydrous MeOH with NaBH4 gave {3-[(3,5-dimethyl-pyridin-2-ylmethyl)-amino]-propyl}-carbamic acid tert-butyl ester as a brown oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07863293B2 |
| Source dataset | uspto-grants-2011_01 |
| ORD ID | ord-c4658868c12a4c62af61ffe28acf8d17 |
| Source note | uspto-grants-2011_01 |