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HRID251096

反应详情

EQUATION

反应方程式

HRID 251096 的结构方程式

REACTANTS

反应物

3
结构：CC(=O)c1ccccn1
HCID14286

1-(2-Pyridyl)-1-ethanone

C7H7NO

结构：CC(C)(C)OC(=O)NCCCN
HCID2735700

N-Boc-1,3-propanediamine

C8H18N2O2

结构：CC(=O)O[BH-](OC(C)=O)OC(C)=O.[Na+]
HCID5049666

Sodium triacetoxyborohydride

C6H10BNaO6

PRODUCTS

生成物

1
结构：CC(NCCCNC(=O)OC(C)(C)C)c1ccccn1
HCID67272175

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：ClCCl
溶剂HCID6344

Dichloromethane

CH2Cl2

PROCEDURE

实验过程

Using General Procedure B: Reaction of 2-acetyl-pyridine and (3-amino-propyl)-carbamic acid tert-butyl ester with NaBH(OAc)3 in CH2Cl2 gave [3-(1-pyridin-2-yl-ethylamino)-propyl]-carbamic acid tert-butyl ester as a colorless oil.