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HRID251214

反应详情

EQUATION

反应方程式

HRID 251214 的结构方程式

REACTANTS

反应物

3
结构：CC(C)(C)OC(=O)N1CCC(N)CC1
HCID1268291

4-Amino-1-Boc-piperidine

C10H20N2O2

结构：CC(=O)O[BH-](OC(C)=O)OC(C)=O.[Na+]
HCID5049666

Sodium triacetoxyborohydride

C6H10BNaO6

结构：O=C1CCCc2cccnc21
HCID11744777

6,7-dihydro-5H-quinolin-8-one

C9H9NO

PRODUCTS

生成物

1
结构：CC(C)(C)OC(=O)N1CCC(NC2CCCc3cccnc32)CC1
HCID67272553

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：ClCCl
溶剂HCID6344

Dichloromethane

CH2Cl2

PROCEDURE

实验过程

Using General Procedure B: Reaction of 6,7-Dihydro-5H-quinolin-8-one and 4-Amino-piperidine-1-carboxylic acid tert-butyl ester with NaBH(OAc)3 in CH2Cl2 gave 4-(5,6,7,8-Tetrahydro-quinolin-8-ylamino)-piperidine-1-carboxylic acid tert-butyl ester as a colorless oil.