huagongshe.com
HRID251227

反应详情

EQUATION

反应方程式

HRID 251227 的结构方程式

REACTANTS

反应物

3
结构：CC(=O)O[BH-](OC(C)=O)OC(C)=O.[Na+]
HCID5049666

Sodium triacetoxyborohydride

C6H10BNaO6

结构：CC(C)(C)[Si](C)(C)OCCCC=O
HCID10888976

4-(tert-butyldimethylsilyloxy)butanal

C10H22O2Si

结构：Cc1cnc(NC2CCCc3cccnc32)c(C)c1
HCID67273035

未命名化合物

PRODUCTS

生成物

1
结构：Cc1cnc(N(CCCCO[Si](C)(C)C(C)(C)C)C2CCCc3cccnc32)c(C)c1
HCID67271684

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：ClCCl
溶剂HCID6344

Dichloromethane

CH2Cl2

PROCEDURE

实验过程

Using General Procedure B, reaction of (3,5-dimethyl-pyridin-2-yl)-(5,6,7,8-tetrahydro-quinolin-8-yl)-amine, 4-(tert-butyl-dimethyl-silanyloxy)-butyraldehyde and NaBH(OAc)3 in CH2Cl2 gave [4-(tert-butyl-dimethyl-silanyloxy)-butyl]-(3,5-dimethyl-pyridin-2-yl)-(5,6,7,8-tetrahydro-quinolin-8-yl)-amine.