HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 58089228, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 86610722 | HCID 86610722 | — |
| Solvent | Ethanol | HCID 702 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 58089228 | HCID 58089228 | 90% |
Reaction Steps
97.5 g of compound 17 (412 mmole) was dissolved in 530 ml EtOH and 1050 ml water. 87 g NaOH (2.19 mole) was added and the mixture was refluxed for 5 hours. Afterwards the mixture was acidified with concentrated HCl to pH 1. The formed precipitate was filtered off and dried under reduced pressure. 82 g was obtained (90% yield).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07863428B2 |
| Source dataset | uspto-grants-2011_01 |
| ORD ID | ord-6919084bb0a146e89da8ea9d1ad33415 |
| Source note | uspto-grants-2011_01 |