HRID251567

反应详情

EQUATION

反应方程式

HRID 251567 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

Add Triethylamine to a solution of Ethyl 4-(3-(2,6-dimethylbenzyloxy)phenyl)-4-bromo-butyrate (Step E) in carbon tetrachloride. After stirring approximately for 4 hours, the mixture can be filtered through a pad of silica gel few times, and concentrate to give the title compound.

WORKUP

后处理

  1. filtrationthe mixture can be filtered through a pad of silica gel few times
  2. concentrationconcentrate