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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 251746Generated: November 1, 2026

Hydrazine hydrate (1:1) → HCID 67268872, compound

https://huagongshe.com/reaction/251746

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHydrazine hydrate (1:1)HCID 24654—
ReactantHCID 523521HCID 523521—
SolventIsopropanolHCID 3776—
ProductHCID 67268872HCID 67268872—

Reaction Conditions

Temperature80 °C

Reaction Steps

The methyl 4-methoxyquinoline-2-carboxylate (1 eq) was dissolved in i-PrOH (0.75 M) and then hydrazine monohydrate (10 eq) was added. The reaction mixture was heated at 80° C. overnight and then the solvent was evaporated under reduced pressure and the crude product was used in the next step without purification. MS (ES) C11H11N3O2 required: 217, found: 218 (M+H)+.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07863294B2
Source datasetuspto-grants-2011_01
ORD IDord-65f1e5d6e90e4349a414f7bd46654e23
Source noteuspto-grants-2011_01