HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 57686831, compound → HCID 57686802, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 57686831 | HCID 57686831 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 57686802 | HCID 57686802 | 98.9% |
Reaction Steps
3-(6-chloroimidazo[1,2-b]pyridazin-2-yl)-5-(2-methoxyethoxy)benzonitrile (10 mmol) in 100 ml MeOH was added Pd/C(1 mmol) and stirred at room temperature for 4 h. Pd-C was removed and the filtrate was concentrated to provide 3-(imidazo[1,2-b]pyridazin-2-yl)-5-(2-methoxyethoxy)benzonitrile (98.9%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07868001B2 |
| Source dataset | uspto-grants-2011_01 |
| ORD ID | ord-cccfd2b0b06444d388973c5b7c980989 |
| Source note | uspto-grants-2011_01 |