HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Azide → HCID 131728611, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Azide | HCID 33557 | — |
| Reactant | HCID 59028001 | HCID 59028001 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 131728611 | HCID 131728611 | — |
Reaction Steps
50.0 mg of the compound of Example 80A and 15.6 mg (0.24 mmol) of sodium azide are stirred in 3 ml of N,N-dimethylformamide in a closed reaction vessel at 90° C. over night. After fine purification by preparative RP-HPLC (Method 6) 46 mg of the target compound are obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07867992B2 |
| Source dataset | uspto-grants-2011_01 |
| ORD ID | ord-03749ae014754cee9f5c13ae3fb77111 |
| Source note | uspto-grants-2011_01 |