HuagongsheHuagongshe Chemistry Print Report · For research reference only
3,5-Difluorobenzaldehyde → HCID 66842583, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3,5-Difluorobenzaldehyde | HCID 588160 | — |
| Reactant | HCID 86597115 | HCID 86597115 | — |
| Product | HCID 66842583 | HCID 66842583 | 27% |
Reaction Steps
This material was prepared from (3,5-dimethoxy-4-1-propylbenzyl)phosphonate and 3,5-difluorobenzaldehyde in 27% yield in the same way as described in Example 21. 1HNMR (CDCl3, ppm): δ 1.32 (d, J=7.0 Hz, 6H), 3.66 (qint., J=7.0 Hz, 1H), 3.90 (s, 6H), 6.72 (s, 2H), 6.8-7.2 (m, 5H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07868047B2 |
| Source dataset | uspto-grants-2011_01 |
| ORD ID | ord-9e2b48e045aa4be1bbf85524109fd7cf |
| Source note | uspto-grants-2011_01 |