HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl 4-methoxybutanoate → HCID 66888453, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl 4-methoxybutanoate | HCID 542317 | — |
| Reactant | 5-Bromo-2-hydrazinopyridine | HCID 11535699 | — |
| Product | HCID 66888453 | HCID 66888453 | — |
Reaction Steps
A mixture of 18.80 g of (5-bromopyridin-2-yl)hydrazine [77992-44-0] and 14.54 g of methyl 4-methoxybutyrate [29006-01-7] is heated to reflux over 16 hours. The reaction solution is subsequently cooled and purified by means of flash chromatography (SiO2 60F). The title compound is identified on the basis of the Rf value.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07868036B2 |
| Source dataset | uspto-grants-2011_01 |
| ORD ID | ord-5ff049fd4acc42c1a6ba190671a246db |
| Source note | uspto-grants-2011_01 |