2-Bromoethyl methyl ether → Methyl 8-(2-methoxyethoxy)naphthalene-2-carboxylate

HRID 252360Notes

Reaction equation

HRID 252360 reaction equation
[OH:1][C:2]1[CH:3]=[CH:4][CH:5]=[C:6]2[C:11]=1[CH:10]=[C:9]([C:12]([O:14][CH3:15])=[O:13])[CH:8]=[CH:7]2.Br[CH2:17][CH2:18][O:19][CH3:20]>>[CH3:20][O:19][CH2:18][CH2:17][O:1][C:2]1[CH:3]=[CH:4][CH:5]=[C:6]2[C:11]=1[CH:10]=[C:9]([C:12]([O:14][CH3:15])=[O:13])[CH:8]=[CH:7]2

Participants

3

Reactant 2

HCID 809722-Bromoethyl methyl etherHCID 22128866Methyl 8-hydroxynaphthalene-2-carboxylate

Product 1

HCID 66888784Methyl 8-(2-methoxyethoxy)naphthalene-2-carboxylate

Procedure

Analogously to method C, 2.02 g of methyl 8-hydroxynaphthalene-2-carboxylate [115399-09-2] and 2.08 g of 1-bromo-2-methoxyethane are reacted. The title compound is identified on the basis of the Rf value.

Sources & evidence

ORD record
ord-6e2f694b91f34bd3b20b3b9c7eee499d
Source dataset
uspto-grants-2011_01
Patent number
US07868036B2

Reaction notes

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