HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 66888418, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 66889038 | HCID 66889038 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 66888418 | HCID 66888418 | — |
Reaction Steps
1.030 g of (R)-3-(1-methoxycarbonyl-1-methyl-ethyl)-piperidine-1-carboxylic acid tert-butyl ester are taken up in 10 ml of 4M HCl in dioxane. The reaction solution is left to stand at room temperature for 1 hour and is then concentrated under reduced pressure to provide the title compound as colourless solid which can be used without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07868036B2 |
| Source dataset | uspto-grants-2011_01 |
| ORD ID | ord-e8a6ff54f6964407a00170b3a372fbae |
| Source note | uspto-grants-2011_01 |