HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 23158638, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Ethyl Thioglycolate | HCID 12185 | — |
| Reactant | HCID 19008558 | HCID 19008558 | — |
| Reactant | HCID 23158640 | HCID 23158640 | — |
| Solvent | 1,2-Dichloroethane | HCID 11 | — |
| Product | HCID 23158638 | HCID 23158638 | — |
Reaction Steps
Ethyl 2-mercaptoacetate (I-A) and ethyl 2-isothiocyanato-ethanesulfonate (I-B) or 2-isothiocyanato-ethanesulfonic acid, alternatively, are dissolved in 1,2-dichloroethane and triethylamine is added. The product ethyl 2-(4-oxo-2-thioxothiazolidin-3-yl)-ethanesulfonate (1-C) can be isolated after e.g. 1 h of stirring and subsequent solvent removement.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07868185B2 |
| Source dataset | uspto-grants-2011_01 |
| ORD ID | ord-ae2d294b728a40f0808b3d08d08acd53 |
| Source note | uspto-grants-2011_01 |