HuagongsheHuagongshe Chemistry Print Report · For research reference only
Morpholine → Pyridine-3-sulfonyl chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Morpholine | HCID 8083 | — |
| Reactant | 5-Bromopyridine-3-sulfonyl chloride | HCID 20324474 | — |
| Product | Pyridine-3-sulfonyl chloride | HCID 3164136 | 13% |
Reaction Steps
Using an analogous method to that described in the portion of Example 8 that is concerned with the preparation of starting materials, 5-bromopyridine-3-sulfonyl chloride was reacted with morpholine to give the required starting material (90 mg, 13% yield from the pyridine-3-sulfonyl chloride); Mass Spectrum: M+H+ 350 and 352.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07868188B2 |
| Source dataset | uspto-grants-2011_01 |
| ORD ID | ord-76d1e5968c5f4e1f8ec5773f376776ee |
| Source note | uspto-grants-2011_01 |