HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 86620386, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 11541283 | HCID 11541283 | — |
| Product | HCID 86620386 | HCID 86620386 | — |
Reaction Steps
Using an analogous procedure to that described in Example 61, N-[5-(6-chloro-5-phenylsulfonylaminopyridin-3-yl)-4-methyl-1,3-thiazol-2-yl]acetamide was hydrolysed with aqueous hydrochloric acid solution to give the title compound; 1H NMR Spectrum: (DMSOd6) 2.11 (s, 3H), 7.24 (s, 2H), 7.50 (d, 1H), 7.60 (m, 2H), 7.68 (m, 1H), 7.77 (d, 2H), 8.14 (s, 1H), 10.42 (br s, 1H); Mass Spectrum: M+H+ 381.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07868188B2 |
| Source dataset | uspto-grants-2011_01 |
| ORD ID | ord-3cd6d75d4699451399dc55f1a7d5e755 |
| Source note | uspto-grants-2011_01 |