HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Cyanobenzenesulfonyl chloride → HCID 86620408, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Cyanobenzenesulfonyl chloride | HCID 39497 | — |
| Reactant | HCID 86244444 | HCID 86244444 | — |
| Product | HCID 86620408 | HCID 86620408 | — |
Reaction Steps
Using an analogous procedure to that described in Example 83, N-[5-(5-aminopyridin-2-yl)-4-methyl-1,3-thiazol-2-yl]acetamide was reacted with 4-cyanophenylsulfonyl chloride to give the title compound; 1H NMR Spectrum: (DMSOd6) 2.14 (s, 3H), 2.48 (s, 3H), 7.57 (m, 2H), 7.94 (d, 2H), 8.07 (d, 2H), 8.26 (m, 1H), 10.86 (br s, 1H), 12.06 (s, 1H); Mass Spectrum: M+H+ 414.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07868188B2 |
| Source dataset | uspto-grants-2011_01 |
| ORD ID | ord-0dbea3e4b23f4877b9105b43cd5e1940 |
| Source note | uspto-grants-2011_01 |