HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → HCID 59736823, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | HCID 59736932 | HCID 59736932 | — |
| Solvent | Triethylamine | HCID 8471 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 59736823 | HCID 59736823 | 41% |
Reaction Steps
Following the same procedure described for Example 48, step 3 (scheme 36) but substituting compound 171 for compound 299 and using ethyl acetate and triethylamine as a solvent instead methanol, the title compound 300 was obtained in 41% yield over two steps. MS: calc: 305.5; found: 306.1 (M+H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07868205B2 |
| Source dataset | uspto-grants-2011_01 |
| ORD ID | ord-0846b8df4f534f3f98e4eb71c173fb66 |
| Source note | uspto-grants-2011_01 |