HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 178518552, compound → HCID 178517909, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 178518552 | HCID 178518552 | — |
| Catalyst | Nickel | HCID 935 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 178517909 | HCID 178517909 | 78% |
Reaction Steps
A mixture of 2-mercapto-5,6,7,8,9,10-hexahydrocycloocta[d]-pyrimidine-4-ol (1 g; 4.76 mmol) and 10 g of Raney nickel in 40 mL of abs. EtOH was refluxed for 5 hours and filtered. The filtrate was evaporated to give 5,6,7,8,9,10-hexahydrocycloocta[d]-pyrimidine-4-ol as a pale-grey solid (0.66 g; 78% yield).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07872000B2 |
| Source dataset | uspto-grants-2011_01 |
| ORD ID | ord-cc3ba456eafe4f85b623fc92bbe2eb8b |
| Source note | uspto-grants-2011_01 |