HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Methylpiperazine → HCID 178480622, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Methylpiperazine | HCID 53167 | — |
| Reactant | 3H-Pyrazolo[4,3-c]quinolin-3-one, 2,5-dihydro- | HCID 317991 | — |
| Product | HCID 178480622 | HCID 178480622 | — |
Reaction Steps
The title compound was prepared following the procedure in Step 5 using 13a and 1-methylpiperazine. 1H-NMR (CD3OD) δ (ppm): 2.44 (3H, s), 2.74 (4H, brm), 3.44 (4H, brm), 7.03 (1H, d, J=2.20 Hz), 7.27 (1H, ddd, J=7.41, 1.64, 1.10 Hz), 7.35 (1H, dd, J=9.07, 2.47 Hz), 7.65 (2H, m), 7.99 (2H, m), 8.17 (1H, d, J=9.07 Hz), 8.53 (1H, s). m/z 360.4 (MH+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07872002B2 |
| Source dataset | uspto-grants-2011_01 |
| ORD ID | ord-d74bb6ca1cc34548aca8cf83e116febc |
| Source note | uspto-grants-2011_01 |