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HRID252954

反应详情

EQUATION

反应方程式

HRID 252954 的结构方程式

REACTANTS

反应物

2
结构：CN1CCNCC1
HCID53167

1-Methylpiperazine

C5H12N2

结构：O=c1[nH][nH]c2c1cnc1ccccc12
HCID317991

3H-Pyrazolo[4,3-c]quinolin-3-one, 2,5-dihydro-

C10H7N3O

PRODUCTS

生成物

1
结构：CN1CCN(c2ccc3c4nn(-c5ccccc5)c(=O)c-4c[nH]c3c2)CC1
HCID178480622

未命名化合物

PROCEDURE

实验过程

The title compound was prepared following the procedure in Step 5 using 13a and 1-methylpiperazine. 1H-NMR (CD3OD) δ (ppm): 2.44 (3H, s), 2.74 (4H, brm), 3.44 (4H, brm), 7.03 (1H, d, J=2.20 Hz), 7.27 (1H, ddd, J=7.41, 1.64, 1.10 Hz), 7.35 (1H, dd, J=9.07, 2.47 Hz), 7.65 (2H, m), 7.99 (2H, m), 8.17 (1H, d, J=9.07 Hz), 8.53 (1H, s). m/z 360.4 (MH+).