HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Methylpiperazine → HCID 178480623, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Methylpiperazine | HCID 53167 | — |
| Reactant | HCID 178507230 | HCID 178507230 | — |
| Reactant | HCID 178515224 | HCID 178515224 | — |
| Product | HCID 178480623 | HCID 178480623 | — |
Reaction Steps
The title compound was prepared following the procedure for 14a using 13b and 1-methylpiperazine. 1H-NMR (CD3OD) δ (ppm): 2.39 (3H, s), 2.67 (4H, brm), 3.40 (4H, brm), 7.01 (1H, d, J=2.47 Hz), 7.34 (1H, dd, J=9.07, 2.47 Hz), 7.46 (2H, dd, J=6.87, 2.20 Hz), 8.09 (2H, dd, J=7.14, 1.92 Hz), 8.19 (1H, d, J=9.07 Hz), 8.51 (1H, s). m/z 394.9 (MH+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07872002B2 |
| Source dataset | uspto-grants-2011_01 |
| ORD ID | ord-09d1db64492e415db47956bc4c366872 |
| Source note | uspto-grants-2011_01 |