Piperidin-4-ol → HCID 178515223, compound

Participants

Reaction Steps

The title compound was prepared following the procedure described in the synthesis of 28a using 27a and 4-hydroxypiperidine. 1H-NMR (DMSO-d6) δ (ppm): 1.54 (2H, brm), 1.87 (2H, brm), 2.85 (2H, brm), 3.20 (1H, m), 3.64 (1H, brm), 4.74 (1H, brd, J=3.84 Hz), 7.10 (1H, m), 7.22 (1H, d, J=7.97 Hz), 7.40 (2H, m), 7.76 (1H, d, J=2.90 Hz), 8.20 (2H, m), 8.64 (1H, s). m/z 379.2 (MH+).

Provenance & Evidence