HRID253422

反应详情

EQUATION

反应方程式

HRID 253422 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

1H-Pyrrolo[2,3-b]pyridine 7-oxide 91 was synthesized by reacting 7-azaindole 6 with an oxidizing agent (e.g. m-CPBA) in a non-reactive solvent (e.g. dimethoxyethane) as described by Schneller, S. W.; Luo, Jiann-Kuan. J. Org. Chem. 1980, 45:4045-4048. The compound was isolated by filtration of the resulting solid that forms upon standing at 5° C. for typically 1-3 h.

WORKUP

后处理

  1. customThe compound was isolated by filtration of the resulting solid that