HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → HCID 11317405, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 11167947 | HCID 11167947 | — |
| Product | HCID 11317405 | HCID 11317405 | 86.6% |
Reaction Steps
In a manner similar to that of Example 2a, by reaction of 300 mg (0.6 mmol) of ethyl 4′-(4-aminobutoxy)-3′-(5,5,8,8-tetramethyl-5,6,7,8-tetrahydronaphth-2-yl)biphenyl-4-carboxylate with 240 mg (6 mmol) of sodium hydroxide. 245 mg of 4′-(4-aminobutoxy)-3′-(5,5,8,8-tetramethyl-5,6,7,8-tetrahydronaphth-2-yl)biphenyl-4-carboxylic acid are obtained in the form of a white solid (m.p.=250° C., yield=86%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07872026B2 |
| Source dataset | uspto-grants-2011_01 |
| ORD ID | ord-ed359faf7a04481daa5244928d60aa53 |
| Source note | uspto-grants-2011_01 |