Sodium Hydroxide → HCID 66842981, compound

Participants

Reaction Steps

Ethyl (2R)-2-amino-4-cyclohexylbutanoate hydrochloride (4.00 g, 18.75 mmol) was dissolved in MeOH/Water (10/5 ml). Sodium hydroxide (1.50 g, 37.50 mmol) was added. The reaction mixture was stirred for 1 h and concentrated to give the title compound as a colourless solid (containing 100 mol % of sodium chloride). 1H NMR [(CD3)2SO), 400 MHz] δ0.83-0.97 (m, 2H), 1.10-1.33 (m, 6H), 1.48-1.78 (m, 7H), 3.15 (dd, 1H).

Provenance & Evidence