HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 66852303, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 10343421 | HCID 10343421 | — |
| Solvent | Isopropanol | HCID 3776 | — |
| Product | HCID 66852303 | HCID 66852303 | — |
Reaction Steps
To a 4.45 g of 1-(4-Methoxybenzenesulfonyl)-3-(4-methylpiperazin-1-ylmethyl)-5-nitro-1H-indole (example-124), was added the saturated solution of hydrochloric acid in isopropyl alcohol and stirred at room temperature till crystalline compound separates out. The compound was isolated by filtration, washed with n-hexane, ethylacetate and dried under vacuum. IR spectra (cm−1): 1159, 1263, 1337, 1372; Mass (m/z): 445 M+H)+
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07875605B2 |
| Source dataset | uspto-grants-2011_01 |
| ORD ID | ord-9ae6ac8ae95549a78ec15c2565bbb820 |
| Source note | uspto-grants-2011_01 |