HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 59321321, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 2,4-Difluoronitrobenzene | HCID 67967 | — |
| Reactant | HCID 178430842 | HCID 178430842 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 59321321 | HCID 59321321 | — |
Reaction Steps
15.9 g (0.1 mol) 2,4-Difluoro-nitrobenzene, 16.5 g 2-Cyclohexyl-4-methylimidazole, 30 g potassium carbonate, and 150 ml acetonitrile were heated 24 hours at 60° C. After cooling the product was filtered off, washed with 100 ml acetonitrile, evaporated to dryness and chromatographed on silica gel with 5% MeOH/CH2Cl2.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07875618B2 |
| Source dataset | uspto-grants-2011_01 |
| ORD ID | ord-c1fcc5a2f58043c3bbd7786ce7001a75 |
| Source note | uspto-grants-2011_01 |