HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 254283Generated: October 30, 2026
HCID 59321321, compound → HCID 66862726, compound
https://huagongshe.com/reaction/254283
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | HCID 59321321 | HCID 59321321 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Nickel | HCID 935 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 66862726 | HCID 66862726 | — |
Reaction Steps
3.03 g 2-(2-Cyclohexyl-4-methyl-imidazol-1-yl)-4-fluoro-nitrobenzene (10 mmol) were dissolved in 50 ml ethanol, 0.5 g Raney-Nickel was added and the mixture was heated 5 hours in a closed vessel at 40-45° C. and 10 bar hydrogen. After cooling the catalyst was removed and the filtrate was distilled to dryness.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US07875618B2 |
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| Source dataset | uspto-grants-2011_01 |
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| ORD ID | ord-c2a018849c254c529a67ca4bec83e17d |
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| Source note | uspto-grants-2011_01 |
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