HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 66863032, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | 1,1'-Carbonyldiimidazole | HCID 68263 | — |
| Reactant | HCID 66862546 | HCID 66862546 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 66863032 | HCID 66863032 | — |
Reaction Steps
1.45 g 4-Chloro-2-(2-cyclohexyl-4-methyl-imidazol-1-yl)-aniline were stirred in 25 ml toluene. 1.0 g Carbonyldiimidazole was added and the mixture was refluxed for 6 hours. After cooling 25 ml water was added, the product was filtered off, washed with 20 ml water and 25 ml toluene and dried.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07875618B2 |
| Source dataset | uspto-grants-2011_01 |
| ORD ID | ord-2c64572a5c214b5ab685f552e054d88e |
| Source note | uspto-grants-2011_01 |