HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Chloro-2-fluoro-1-nitrobenzene → 1-(2,5-Dichlorophenyl)-3,4-dimethylimidazo[1,5-a]quinoxaline
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Chloro-2-fluoro-1-nitrobenzene | HCID 69691 | — |
| Reactant | 1-(2,5-Dichlorophenyl)-8-fluoro-3,4-dimethylimidazo[1,5-a]quinoxaline | HCID 42629229 | — |
| Product | 1-(2,5-Dichlorophenyl)-3,4-dimethylimidazo[1,5-a]quinoxaline | HCID 42629478 | 30% |
Reaction Steps
1-(2,5-Dichlorophenyl)-3,4-dimethylimidazo[1,5-a]quinoxaline was synthesized in a manner similar to 1-(2,5-dichlorophenyl)-8-fluoro-3,4-dimethylimidazo[1,5-a]quinoxaline starting with 2-fluoro-4-chloronitrobenzene. A white solid was recovered (0.04 g) 30% yield. MS (ES) m/z 342.0 [M+1]+
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07875618B2 |
| Source dataset | uspto-grants-2011_01 |
| ORD ID | ord-230094960cb046d79e732c95be49b2c7 |
| Source note | uspto-grants-2011_01 |