HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethylenediamine → HCID 58951787, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethylenediamine | HCID 3301 | — |
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | 2,3-Dimethyl-4-methoxyphenylacetonitrile | HCID 594894 | — |
| Product | HCID 58951787 | HCID 58951787 | — |
| Product | HCID 66855993 | HCID 66855993 | — |
Reaction Steps
rac-2-(4-Methoxy-2,3-dimethyl-phenyl)-propionitrile which was prepared from 2-(4-methoxy-2,3-dimethyl-phenyl)-acetonitrile and methyl iodide in analogy to Example 65a) was reacted with ethylenediamine to form rac-2-[1-(4-methoxy-2,3-dimethyl-phenyl)-ethyl]-4,5-dihydro-1H-imidazole in analogy to Example 19b; isolated as hydrochloride: white powder; MS (EI): 233.3 ((M+.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07875645B2 |
| Source dataset | uspto-grants-2011_01 |
| ORD ID | ord-917333c3fd0f490183d9fb20a412fb32 |
| Source note | uspto-grants-2011_01 |