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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 254564Generated: October 27, 2026

p-Toluenesulfonic acid → HCID 178448987, compound

https://huagongshe.com/reaction/254564

Reaction equation

Participants

RoleNameHCIDCharge
Reactantp-Toluenesulfonic acidHCID 6101—
ReactantButylamineHCID 8007—
Reactant2-Chloro-3,6-difluorobenzaldehydeHCID 2773509—
ProductHCID 178448987HCID 178448987—

Reaction Steps

Butyl-[1-(2-chloro-3,6-difluoro-phenyl)-meth-(E)-ylidene]-amine was prepared from 2-chloro-3,6-difluorobenzaldehyde, N-butylamine and p-toluenesulphonic acid in analogy to Example 191a): yellow oil; MS (ISP): 234.1 ([M+H]+, 30%), 232.3 ([M+H]+, 100%).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07875645B2
Source datasetuspto-grants-2011_01
ORD IDord-3f29a09a77a44ddd9a298969c82bdc48
Source noteuspto-grants-2011_01