HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethylacetate heptane → 2-Ethyl-3,6-difluoro-benzaldehyde
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethylacetate heptane | HCID 21899848 | — |
| Reactant | HCID 178448986 | HCID 178448986 | — |
| Product | 2-Ethyl-3,6-difluoro-benzaldehyde | HCID 58951902 | — |
Reaction Steps
2-Ethyl-3,6-difluoro-benzaldehyde was prepared from butyl-[1-(2-ethyl-3,6-difluoro-phenyl)-meth-(E)-ylidene]-amine by flash chromatography (silica gel, ethyl acetate/heptane gradient): yellow oil; 1H-NMR (CDCl3): 1.22 (3H, t, CH3), 3.02 (2H, m, CH2), 6.99 (1H, ddd, ArH), 7.23 (1H, ddd, ArH), 10.45 (1H, d, CH═O).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07875645B2 |
| Source dataset | uspto-grants-2011_01 |
| ORD ID | ord-b0192905c2dd4bbb950f289d8ded8df9 |
| Source note | uspto-grants-2011_01 |