Trichloroisocyanuric Acid → HCID 24779851, compound

HRID 254575Notes

Reaction equation

HRID 254575 reaction equation
[CH2:1]([C:3]1[C:14]([F:15])=[CH:13][CH:12]=[C:11]([CH2:16][CH3:17])[C:4]=1[CH2:5][C:6]1[NH:7][CH2:8][CH2:9][N:10]=1)[CH3:2].C1(N(Cl)C(=O)N(Cl)C(=O)N1Cl)=O.C1CCN2C(=NCCC2)CC1>>[CH2:1]([C:3]1[C:14]([F:15])=[CH:13][CH:12]=[C:11]([CH2:16][CH3:17])[C:4]=1[CH2:5][C:6]1[NH:10][CH:9]=[CH:8][N:7]=1)[CH3:2]

Participants

4

Reactant 3

HCID 6909Trichloroisocyanuric AcidHCID 811841,8-Diazabicyclo(5.4.0)undec-7-eneHCID 58951699HCID 58951699, compound

Product 1

HCID 24779851HCID 24779851, compound

Procedure

2-(2,6-Diethyl-3-fluoro-benzyl)-1H-imidazole was prepared from 2-(2,6-diethyl-3-fluoro-benzyl)-4,5-dihydro-1H-imidazole (Example 197), TCCA and DBU in analogy to Example 194e): light yellow crystals; MS (ISP): 233.3 ([M+H]+).

Sources & evidence

ORD record
ord-83dbcac614bc43b58366c357f545b05c
Source dataset
uspto-grants-2011_01
Patent number
US07875645B2

Reaction notes

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