Trichloroisocyanuric Acid → HCID 58951825, compound

HRID 254576Notes

Reaction equation

HRID 254576 reaction equation
[Cl:1][C:2]1[C:3]([CH2:16][CH3:17])=[C:4]([C:11]([CH2:14][CH3:15])=[CH:12][CH:13]=1)[CH2:5][C:6]1[NH:7][CH2:8][CH2:9][N:10]=1.C1(N(Cl)C(=O)N(Cl)C(=O)N1Cl)=O.C1CCN2C(=NCCC2)CC1>>[Cl:1][C:2]1[C:3]([CH2:16][CH3:17])=[C:4]([C:11]([CH2:14][CH3:15])=[CH:12][CH:13]=1)[CH2:5][C:6]1[NH:10][CH:9]=[CH:8][N:7]=1

Participants

4

Reactant 3

HCID 6909Trichloroisocyanuric AcidHCID 811841,8-Diazabicyclo(5.4.0)undec-7-eneHCID 24779849HCID 24779849, compound

Product 1

HCID 58951825HCID 58951825, compound

Procedure

2-(3-Chloro-2,6-diethyl-benzyl)-1H-imidazole was prepared from 2-(3-chloro-2,6-diethyl-benzyl)-4,5-dihydro-1H-imidazole (Example 196), TCCA and DBU in analogy to Example 194e): light yellow crystals; MS (ISP): 251.3 ([M+H]+, 39%), 249.2 ([M+H]+, 100%).

Sources & evidence

ORD record
ord-b6420a1b26ec4dd8a45fae7515079680
Source dataset
uspto-grants-2011_01
Patent number
US07875645B2

Reaction notes

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