HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trichloroisocyanuric Acid → 2-(3-Chloro-2-ethyl-6-fluoro-benzyl)-1H-imidazole
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trichloroisocyanuric Acid | HCID 6909 | — |
| Reactant | 1,8-Diazabicyclo(5.4.0)undec-7-ene | HCID 81184 | — |
| Reactant | 2-(3-Chloro-2-ethyl-6-fluoro-benzyl)-4,5-dihydro-1H-imidazole | HCID 24779850 | — |
| Product | 2-(3-Chloro-2-ethyl-6-fluoro-benzyl)-1H-imidazole | HCID 58951758 | — |
Reaction Steps
2-(3-Chloro-2-ethyl-6-fluoro-benzyl)-1H-imidazole was prepared from 2-(3-chloro-2-ethyl-6-fluoro-benzyl)-4,5-dihydro-1H-imidazole (Example 198), TCCA and DBU in analogy to Example 194e): light yellow crystals; MS (ISP): 241.2 ([M+H]+, 58%), 239.2 ([M+H]+, 100%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07875645B2 |
| Source dataset | uspto-grants-2011_01 |
| ORD ID | ord-348278992a094d91904c1c1453a0cfa2 |
| Source note | uspto-grants-2011_01 |