HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trichloroisocyanuric Acid → 2-(2-Ethyl-3,6-difluoro-benzyl)-1H-imidazole
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trichloroisocyanuric Acid | HCID 6909 | — |
| Reactant | 1,8-Diazabicyclo(5.4.0)undec-7-ene | HCID 81184 | — |
| Reactant | 2-(2-Ethyl-3,6-difluoro-benzyl)-4,5-dihydro-1H-imidazole | HCID 58951748 | — |
| Product | 2-(2-Ethyl-3,6-difluoro-benzyl)-1H-imidazole | HCID 58951903 | — |
Reaction Steps
2-(2-Ethyl-3,6-difluoro-benzyl)-1H-imidazole was prepared from 2-(2-ethyl-3,6-difluoro-benzyl)-4,5-dihydro-1H-imidazole (Example 199), TCCA and DBU in analogy to Example 194e): light yellow crystals; MS (ISP): 223.3 ([M+H]+, 100%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07875645B2 |
| Source dataset | uspto-grants-2011_01 |
| ORD ID | ord-c6c090c1521145b6b0c9d434f473af87 |
| Source note | uspto-grants-2011_01 |