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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 254585Generated: October 26, 2026

p-Toluenesulfonic acid → HCID 178448989, compound

https://huagongshe.com/reaction/254585

Reaction equation

Participants

RoleNameHCIDCharge
Reactantp-Toluenesulfonic acidHCID 6101—
ReactantButylamineHCID 8007—
Reactant2,6-Difluoro-4-methoxybenzaldehydeHCID 3703713—
ProductHCID 178448989HCID 178448989—

Reaction Steps

Butyl-[1-(2,6-difluoro-4-methoxy-phenyl)-meth-(E)-ylidene]-amine was prepared from 2,6-difluoro-4-methoxybenzaldehyde, N-butylamine and p-toluenesulphonic acid in analogy to Example 186a): yellow oil; MS (ISP): 228.4 ([M+H]+, 100%).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07875645B2
Source datasetuspto-grants-2011_01
ORD IDord-89ca1caf69ef4874afa0b8ff8cae7330
Source noteuspto-grants-2011_01