HRID254911

反应详情

EQUATION

反应方程式

HRID 254911 的结构方程式

PROCEDURE

实验过程

Alternatively, the compound 2 can be obtained by reacting 4-benzyloxy-2-hydroxybenzaldehyde with a mixture of MTPPB and t-BuOK, followed by reaction with 2-bromo-4′-methoxyacetophenone, and the resultant mixture, instead of being subjected to purification to afford compound 2a, was continuously reacted with a mixture of MTPPB and t-BuOK in THF, giving a one pot yield of 74%.

WORKUP

后处理

  1. customthe resultant mixture, instead of being subjected to purification