反应详情

温度

80 °C

A mixture of 2-chlorocyclopentanone (5.00 g, 39.5 mmol) and thiourea (3.00 g, 39.5 mmol) was heated at 80° C. for 3-4 minutes. After cooling to room temperature, the mixture was triturated with ethanol and the solid was collected by filtration to afford the title compound. MS (ESI) m/z 141 (M+H)+.

1. temperatureAfter cooling to room temperature
2. customthe mixture was triturated with ethanol
3. filtrationthe solid was collected by filtration