참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | 2-Chlorocyclopentanone | HCID 12751 | — |
| 반응물 | Thiourea | HCID 2723790 | — |
| 생성물 | 5,6-Dihydro-4H-cyclopenta[d]thiazol-2-amine hydrochloride | HCID 16253246 | — |
반응 단계
A mixture of 2-chlorocyclopentanone (5.00 g, 39.5 mmol) and thiourea (3.00 g, 39.5 mmol) was heated at 80° C. for 3-4 minutes. After cooling to room temperature, the mixture was triturated with ethanol and the solid was collected by filtration to afford the title compound. MS (ESI) m/z 141 (M+H)+.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US07875639B2 |
|---|
| 출처 데이터셋 | uspto-grants-2011_01 |
|---|
| ORD ID | ord-68e40f2e96ba47dab34674e11ed228d7 |
|---|
| 출처 메모 | uspto-grants-2011_01 |
|---|
