反应详情

This compound was prepared as described in Example 54: 2.7 g (0.006 mol) of product of Example 60, 0.65 g (0.006 mol) of triethylamine and 0.12 g of Pd/C (10%) in 30 mol of ethanol were reacted affording an oil residue which was kugelrohr distilled at 80 Pa, pot temperature 104° C., to give 2.07 g (89.8%) of product as a white solid; mp 53°-55° C.

1. customThis compound was prepared
2. customaffording an oil residue which
3. distillationwas kugelrohr distilled at 80 Pa, pot temperature 104° C.