HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → HCID 70450173, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | Methylamine | HCID 6329 | — |
| Reactant | HCID 13361971 | HCID 13361971 | — |
| Product | HCID 70450173 | HCID 70450173 | — |
Reaction Steps
14.7 g of 3,4-dichlorophenylhydroxymalonic acid dimethyl ester were dissolved in 100 ml of methanol, and methylamine was passed in at 60° C. for 1 hour. The mixture was concentrated completely and the crystalline residue was recrystallised from 100 ml of ethanol. 12 g of 3,4-dichlorophenylhydroxymalonic acid dimethylamide (melting point=158°-160° C.) were obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04698333 |
| Source dataset | uspto-grants-1987_10 |
| ORD ID | ord-a16eeed6aff444b8b8b920f2ee6fae92 |
| Source note | uspto-grants-1987_10 |