HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl 6-hydroxy-7-(prop-2-en-1-yl)-1H-indole-2-carboxylate → HCID 20183534, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl 6-hydroxy-7-(prop-2-en-1-yl)-1H-indole-2-carboxylate | HCID 13203765 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 20183534 | HCID 20183534 | — |
Reaction Steps
The product of step b) was dissolved in dry ethanol (350 ml), treated with 10% Pd/C (0.3 g) and hydrogenated at 35 psi at room temperature until H2 uptake ceased (1.5 hours). The catalyst was filtered off and the filtrate evaporated to dryness.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04698345 |
| Source dataset | uspto-grants-1987_10 |
| ORD ID | ord-15372c7080454dc689a6f0ecb4b3b457 |
| Source note | uspto-grants-1987_10 |