Phenethylamine → HCID 13958341, compound

HRID 255525Notes

Reaction equation

HRID 255525 reaction equation
Cl[C:2]1[C:11]2[C:6](=[CH:7][CH:8]=[CH:9][CH:10]=2)[N:5]=[CH:4][C:3]=1[N+:12]([O-:14])=[O:13].[C:15]1([CH2:21][CH2:22][NH2:23])[CH:20]=[CH:19][CH:18]=[CH:17][CH:16]=1>>[N+:12]([C:3]1[CH:4]=[N:5][C:6]2[C:11]([C:2]=1[NH:23][CH2:22][CH2:21][C:15]1[CH:20]=[CH:19][CH:18]=[CH:17][CH:16]=1)=[CH:10][CH:9]=[CH:8][CH:7]=2)([O-:14])=[O:13]

Participants

3

Reactant 2

HCID 1001PhenethylamineHCID 112758084-Chloro-3-nitroquinoline

Product 1

HCID 13958341HCID 13958341, compound

Procedure

Using the method of Example 1, 4-chloro-3-nitroquinoline was reacted with 2-(phenyl)ethylamine to provide yellow solid 3-nitro-4-[2-(phenyl)ethylamino]quinoline, the melting point of the crude product being 174°-180° C.

Sources & evidence

ORD record
ord-a2b2dd41e3944fbe9648a43e80682e8a
Source dataset
uspto-grants-1987_10
Patent number
US04698348

Reaction notes

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